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Category Archives: Analytical Chemistry and New Analytical Methods

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A Validated RP- HPLC Method for the Simultaneous Estimation of Empagliflozin and Linagliptin in its Bulk and Pharmaceutical Dosage Forms

Jayalaxmi1, Dr. T. Rajesh1, Dr. Gampa Vijaya Kumar*2 1KGR Institute of Technology and Management, Rampally, Kesara, Rangareddy, Telangana, India. 2Professor and Head, Department of Pharmacy, KGR Institute of Technology and Management, Rampally, Kesara, Rangareddy, Telangana, India. A B S T R A C T A new method was established for simultaneous estimation of Empagliflozin and Linagliptin by RP-HPLC method. The ... Read More »

A Validated RP-HPLC Method Development and Validation for Sacubitril and Valsartan in Combine Pharmaceutical Dosage Forms

Sarada1, P. Sowjanya2, Dr. Gampa Vijaya Kumar*3 1,2KGR Institute of Technology and Management, Rampally, Kesara, Rangareddy, Telangana, India, 3Professor and Head, Dept. of Pharmacy, KGR Institute of Technology and Management, Rampally, Kesara, Rangareddy, Telangana, India. A B S T R A C T The Present work was to develop a simple, fast, accurate, precise, reproducible, Reverse Phase High Performance Liquid ... Read More »

Analytical Method Development and Validation for Elbasvir and Grazoprevir in Combine Phaarmaceutical Dosage forms by RP-HPLC

Abilash Reddy Vancha1, Dr. D. Naresh1, P. Sowjanya1, Dr. Gampa Vijaya Kumar*2 1KGR Institute of Technology and Management, Rampally, Kesara, Rangareddy, Telangana, India. 2Professor and Head, Department of Pharmacy, KGR Institute of Technology and Management, Rampally, Kesara, Rangareddy, Telangana, India A B S T R A C T HPLC is at present one of the most sophisticated tool of the ... Read More »

Analytical Method Development and Validation for the Simultaneous Estimation of Darunavir and Cobicistat by RP-HPLC Method in Bulk and Pharmaceutical Dosage Form

Sd. Asra Ayesha*, G. Devika Subramaniyan Bomma Institute of Pharmacy, Allipuram, Khammam, Telangana, India A B S T R A C T A new, simple, precise, accurate and reproducible RP-HPLC method for simultaneous estimation of Darunavir and Cobicistat in bulk and pharmaceutical formulations was developed. Separation of Darunavir and Cobicistat was successfully achieved on C18 ODS(250mm x 4.6 mm), 5µm., ... Read More »

Analytical Method Development and Validation for the Estimation of Erlotinib Hydrochloride by RP-HPLC Method in Bulk and Pharmaceutical Dosage Form

Gobala Krishnan P*, Munisekhar V, Ranjit Singh B. Rathore Department of Pharmaceutical Chemistry, Vagdevi college of Pharmacy & Research centre, Nellore, Andhra Pradesh, India. A B S T R A C T The chromatographic conditions were successfully developed for the separation of Erlotinib hydrochloride by using the HPLC method for Erlotinib hydrochloride as per ICH Guide lines. Shimadzu LC-2010 series ... Read More »

Simultaneous Estimation Method for the Determination of Rosuvastatin and Ezetimibe from their Combination Tablet Dosage form Using RP-HPLC

S. Mehboob Basha, Shaik Mohmmed Yusuf*, Vummadi Sai Chandana, Bumireddy Pavani, E. Vijay Kumar Department of Pharmaceutical Analysis, Srinivasa Institute of Pharmaceutical Sciences, Proddatur, YSR Kadapa, A.P. India A B S T R A C T Rosuvastatin is an HMG Co-A inhibitor and Ezetimibe is an intestinal cholesterol absorption inhibitor. The combination formulation is used for the treatment of hypercholestrolemia. A ... Read More »

Validated RP-HPLC Method for Simultaneous Estimation of Metformin and Vildagliptin in Its Tablets

Karem Kishore Kumar Reddy, Shaik Mohammed Yusuf*, E. Vijay Kumar, Bumireddy Pavani, E. Divya, Vummadi Sai Chandana Department of Pharmaceutical Analysis, Srinivasa Institute of Pharmaceutical Sciences, Proddatur, YSR Kadapa, A.P. India A B S T R A C T A simple, rapid, sensitive and robust reversed phase-HPLC method was developed and validated to measure simultaneously the amount of Metformin and Vildagliptin ... Read More »

Anti-Diabetic Effect of Diospyros Malabarica against Alloxan Induced Diabetes in Rats

A. Ravi Kumar1*, P. Vengalrao1, S. Satyanarayana1, Gireesh Jampana1, Matle Naga Priyanka2 1Celon Laboratories Private Limited, Aleap Industrial Estate, Gajularamaram, R.R. Dist., Telgana-500090 2Department of Pharmaceutical Analysis Narayana Pharmacy College, Nellore, Andhra Pradesh, India A B S T R A C T The Present study was under taken to evaluation of anti-diabetic potential of Diospyros malabarica(DM) leaves in low dose ... Read More »

Analytical Method Development and Validation for the Simultaneous Estimation of Candesartan cilexitil and Hydrochlorothiazide by RP-HPLC Method in Bulk and Pharmaceutical Dosage Form

Idavalapati Chandana*, M. Gobinath, V. Haribaskar, Ramesh Dhani Department of Pharmaceutical Analysis, Ratnam Institute of Pharmacy, Pidathapolur, Nellore, Andhra Pradesh, India A B S T R A C T The chromatographic conditions were successfully developed for the separation of Candesartan cilexitil and Hydrochlorothiazide  by using zodiac sil C18 Column (150mm x 4.6mm)5µm, flow rate was 1ml/min, mobile phase ratio was ... Read More »

Development and Validation of a New RP-HPLC method for the simultaneous estimation of Sulfamethoxazole sodium and Trimethoprim in finished tablet dosage form

K. Satish*1, V. Karthik Varma2, A. Sunil Kumar3, Kranthi Ponugoti4, J. Karthik5 1,2, 3Department of Pharmaceutical Analysis and Quality Assurance, Vikas College of Pharmaceutical Sciences, Rayanigudem, Suryapet-508376, Telangana, India. 4Department of Pharmacology, Malla Reddy College of Pharmacy, Kompally, Hyderabad-500043, India. 5Department of Pharmceutical Chemistry, Madhira Institute of Technology and Sciences, Madhira Nagar, Chilkur, Nalgonda, Kodad-508206, Telangana, India. A B S T ... Read More »

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